Synthesis and Performance Evaluation of a Cement Retardant AID for Oil Well

Lu Ya; Li Ming; Yang Yan; Guo Zihan; Guo Xiaoyang

doi:10.11911/syztjs.201506008

Volume 43 Issue 6

Nov. 2015

Turn off MathJax

Article Contents

Abstract

References

Petroleum Drilling Techniques > 2015 > 43(6): 40-45. > DOI: 10.11911/syztjs.201506008

Lu Ya, Li Ming, Yang Yan, Guo Zihan, Guo Xiaoyang. Synthesis and Performance Evaluation of a Cement Retardant AID for Oil Well[J]. Petroleum Drilling Techniques, 2015, 43(6): 40-45. DOI: 10.11911/syztjs.201506008

Citation:

PDF (1137 KB)

Synthesis and Performance Evaluation of a Cement Retardant AID for Oil Well

Lu Ya¹,
Li Ming^1,2,
Yang Yan³,
Guo Zihan¹,
Guo Xiaoyang^1,2, ,

1.
School of Material Science and Engineering, Southwest Petroleum University, Chengdu, Sichuan, 610500, China;
2.
State Key Laboratory of Oil and Gas Reservoir Geology and Exploitation, Southwest Petroleum University, Chengdu, Sichuan, 610500, China;
3.
Drilling & Production Technology Research Institute, PetroChina Jidong Oilfield Company, Tangshan, Hebei, 063000, China

More Information

Received Date: December 22, 2014
Revised Date: August 14, 2015

Graphical Abstract

Abstract

Abstract

Because the binary-copolymer cement retardant that is currently used has poor thermal stability, and the component acrylamide(AM) in terpolymer retardant tends to decompose at high temperature,the AM has been replaced with N,N-dimethylacrylamide(DMAM), and three monomers were selected, including 2-acrylamide-2-methyl acrylic acid(AMPS), itaconic acid(IA)and DMAM, by which a terpolymeric retardant AID was synthesized according to the polymerization principle of free radical aqueous solution.The structure and thermal stability of AID were analyzed by gel permeation chromatography (GPC), infrared (IR) spectrometry and thermal weight loss test, which evaluated the performance and the effect on cement compressive strength. Test results showed that AID had better thermal stability and it could resist 355 ℃, in which the mass ratio of AMPS, IA and DMAM was 10:4:1, the reaction temperature was 60 ℃,the dosage of the initiator was 2.0%, with excellent synthetic effect in the reaction time of five hours. The thickening time of the slurry with 0.5% AID is over two times of that without adding AID. When the AID quantity was the same, the slurry thickening time in the range of 90-150 ℃ was over 300 min, and the cement strength developed over 14 MPa. The studies showed that the retardant AIDcould extend the slurry thickening time significantly, and possess strong temperature adaptability, but have no obvious impact on the compressive strength of set cement, which indicates that it can be used widely in the future.
- oil well cement,
- retardant,
- terpolymer,
- deep well,
- well cementing

FullText(HTML)

References (18)

References

[1]	董文博.高温油井水泥缓凝剂的研制[D].成都:西南石油大学材料科学与工程学院,2012. Dong Wenbo.Development of high-temperature oil well cement retarder[D].Chengdu:Southwest Petroleum University,School of Materials Science and Engineering,2012.
[2]	汪世国,张毅,余加水,等.莫深1井抗高温密度水基钻井液体系室内研究[J].新疆石油科技,2006,16(3):9-12,30. Wang Shiguo,Zhang Yi,Yu Jiashui,et al.Indoor research of anti-high temperature density water-based drilling fluid system in Well Moshen 1[J].Xinjiang Petroleum Science Technology,2006,16(3):9-12,30.
[3]	Guo Shenglai,Bu Yuhuan,Shen Zhonghou,et al.The effect of synthesis conditions on the performance of large temperature difference retarder[J].Research Journal of Applied Sciences,Engineering Technology,2013,5(19):4751-4756.
[4]	赵琥,田野,王清顺,等.新型高温缓凝剂PC-H42L的室内合成与评价[J].长江大学学报:自然科学版,2012, 9(7):73-74. Zhao Hu,Tian Ye,Wang Qingshun,et al.Laboratory synthesis and evaluation of a new high-temperature retarder PC-H42L[J].Journal of Yangtze University:Natural Science Edition,2012,9(7):73-74.
[5]	刘景丽,王野,李淑陶,等.高温油井水泥缓凝剂ZH-8的合成及评价[J].钻井液与完井液,2011,28(3):53-55. Liu Jingli,Wang Ye,Li Shutao,et al.Synthesis and evaluation of ultra-high temperature retarder ZH-8 for oil well cement[J].Drilling Fluid Completion Fluid,2011,28(3):53-55.
[6]	刘崇建,黄柏宗,徐同台,等.油气井注水理论与运用[M].北京:石油工业出版社,2001:84-89. Liu Chongjian,Huang Baizong,Xu Tongtai,et al.Theory and application of water injection wells[M].Beijing:Petroleum Industry Press,2001:84-89.
[7]	Eoff L S,Buster D.High temperature synthetic cement retarder[R].SPE 28957,1995.
[8]	Qi Zhigang,Zhu Xiaoming,Cao Huilian.Applications and study on organophosphate acids(salts)for oil well cement retarder[J].Energy Science and Technology,2013,6(2):79-83.
[9]	Brothers L E,Lindsey D W,Terry D T.Set retarded cement compositions and methods for well cementing:US,4941536[P].1990-07-17.
[10]	赵常青,张成金,孙海芳,等.油井水泥宽温带缓凝剂SD210L的研制与应用[J].天然气工业,2013,33(1):90-94. Zhao Changqing,Zhang Chengjin,Sun Haifang,et al.Development and application of the well cement retarder SD210L with a wide high temperature range[J].Natural Gas Industry,2013,33(1):90-94.
[11]	严思明,张长思,杨光,等.新型高温油井缓凝剂HN-2的合成及性能评价[J].化工中间体,2012(10):45-50. Yan Siming,Zhang Changsi,Yang Guang,et al.Synthesis and performance evaluation of the new high-temperature oil cement retarder(HN-2)[J].Chemical Intermediate,2012(10):45-50.
[12]	李勇,曹智,罗杨,等.抗高温油井水泥缓凝剂及其制备方法:中国,201010255859.9[P].2011-02-09. Li Yong,Cao Zhi,Luo Yang,et al.High temperature oil well cement retarder and preparation method:CN,201010255859.9[P].2011-02-09.
[13]	岳家平,徐翔,李早元,等.高温大温差固井水泥浆体系研究[J].钻井液与完井液,2012,29(2):59-62. Yue Jiaping,Xu Xiang,Li Zaoyuan,et al.Research on high temperature and large temperature difference cement slurry system[J].Drilling Fluid Completion Fluid,2012,29(2):59-62.
[14]	郭锦棠,刘建军,靳建洲,等.新型固井水泥高温缓凝剂HTR-200C的性能研究[J].天津大学学报,2012,45(6):529-533. Guo Jintang,Liu Jianjun,Jin Jianzhou,et al.Performance of new high temperature retarder HTR-200C for oil-well cement[J].Journal of Tianjin University,2012,45(6):529-533.
[15]	郭锦棠,夏修建,刘硕琼,等.适用于长封固段固井的新型高温缓凝剂HTR-300L[J].石油勘探与开发,2013,40(5):611-615. Guo Jintang,Xia Xiujian,Liu Shuoqiong,et al.A high temperature retarder HTR-300L used in long cementing interval[J].Petroleum Exploration and Development,2013,40(5):611-615.
[16]	李晓岚,王中华,陈道元,等.抗高温油井水泥缓凝剂的研究进展[J].精细与专用化学品,2011,19(6):33-38. Li Xiaolan,Wang Zhonghua,Chen Daoyuan,et al.Research progress of well cement retarder with high temperature-resistant capacity[J].Fine and Specialty Chemicals,2011,19(6):33-38.
[17]	American Petroleum Institute.API specification 10A:specification for cements and materials for well cementing[S].23rd ed.2002.
[18]	SY/T 5504.1—2005 油井水泥外加剂评价方法(1):缓凝剂[S]. SY/T 5504.1—2005 Oil well cement additives evaluation method:part 1:retarder[S].

[1]	QIN Jianyu, LI Bo, RAO Zhihua, JIN Yong, ZHANG Yong, LIU Yongfeng. Key Cementing Technologies for an Ultra-Deep Extended Reach Well in Enping 21–4 Oilfield, Eastern South China Sea[J]. Petroleum Drilling Techniques, 2025, 53(2): 30-37. DOI: 10.11911/syztjs.2025026
[2]	ZENG Yijin. Novel Advancements and Development Suggestions of Cementing Technologies for Deep and Ultra-Deep Wells of Sinopec[J]. Petroleum Drilling Techniques, 2023, 51(4): 66-73. DOI: 10.11911/syztjs.2023035
[3]	CHEN Lei, YANG Hongqi, XIAO Jingnan, ZHOU Shiming, CHU Yongtao, WEI Zhao. Ultra-Low Density Hollow Microspheres-Nitrogen Foamed Cementing Technology in Block Hangjinqi[J]. Petroleum Drilling Techniques, 2018, 46(3): 34-38. DOI: 10.11911/syztjs.2018049
[4]	LI Jianshan. Challenges and Countermeasures of Well Cementing Operations for Horizontal Wells in the Jinghe Oilfield[J]. Petroleum Drilling Techniques, 2017, 45(6): 19-23. DOI: 10.11911/syztjs.201706004
[5]	Zhu Bing, Nie Yuzhi, Qiu Zailei, Wang Haoren, Chen Hongzhuang, Ma Peng. Research on Fluid Loss Additives of AMPS/DMAM/AA in Well Cementing[J]. Petroleum Drilling Techniques, 2014, 42(6): 40-44. DOI: 10.11911/syztjs.201406008
[6]	Guo Wenmeng, Dang Donghong, Zhu Zexin, Xu Minghui, Chen Guang, Huang Xia. Cementing Techniques of Mono-Bore Well Completion in Yishan Slope of Ordos Basin[J]. Petroleum Drilling Techniques, 2014, 42(4): 75-78. DOI: 10.3969/j.issn.1001-0890.2014.04.014
[7]	Jiao Shaoqing, Zhou Huisheng, Tu Maochuan, Li Zaoyuan, Guo Xiaoyang. Application of Double-Effect Antiwearing Technology in Deep Well X202,Western Sichuan[J]. Petroleum Drilling Techniques, 2013, 41(6): 78-81. DOI: 10.3969/j.issn.1001-0890.2013.06.015
[8]	Jiang Zengdong, Wang Guanglei, Wang Wanjun, Yue Ting, Lu Shifen. Development of Cementing Evaluation Equipment DCX for Flushing Efficiency[J]. Petroleum Drilling Techniques, 2013, 41(3): 127-129. DOI: 10.3969/j.issn.1001-0890.2013.03.025
[9]	Liang Erguo, Li Zifeng, Wang Changjin, Han Dongying. Casing Abrasion Prediction for Deep and Extended Reach Wells[J]. Petroleum Drilling Techniques, 2013, 41(2): 65-69. DOI: 10.3969/j.issn.1001-0890.2013.02.013
[10]	Yao Yong, Yin Zongguo, Jiao Jianfang, Guo Guangping, Hong Shaoqing. Cementing with Ultra-High Density Slurry in Well Guanshen-1[J]. Petroleum Drilling Techniques, 2013, 41(1): 118-122. DOI: 10.3969/j.issn.1001-0890.2013.01.023

Cited By

Cited by

Periodical cited type(8)

1.	唐力辉，吴浩，高亚军，王振鹏，谢晓庆，王守磊. 多层非均质水驱油藏分层配注方法研究. 石油化工应用. 2025(03): 51-55+90 .
2.	王群一，马晓丽，蒋明洁，李丹，毕永斌，顾潇. 高地层倾角油藏高低部位油井液量配比研究. 科学技术与工程. 2024(02): 538-544 .
3.	吴宽宽，冯其红，张先敏，孙红霞，于金彪，易红霞. 多层水驱油藏均衡驱替注采参数协同优化方法. 油气地质与采收率. 2023(05): 67-75 .
4.	葛丽珍，孟智强，祝晓林，岳宝林，朱志强. 气顶边水油藏中后期开发调整三维物理模拟研究. 石油钻探技术. 2023(06): 85-92 . 本站查看
5.	张静，郑彬，李红英，刘玉娟，闫志明. 厚油层注采井间注入水纵向波及程度定量研究. 石油钻探技术. 2022(02): 118-125 . 本站查看
6.	葛丽珍，王公昌，张瑞，张烈，张俊廷. 渤海S油田高含水期强水淹层避射原则研究. 石油钻探技术. 2022(03): 106-111 . 本站查看
7.	秦立峰，陈民锋，付世雄，荣金曦. 弹塑性油藏注采渗流场分布及储量有效动用规律. 油气地质与采收率. 2022(03): 128-136 .
8.	赖书敏，赵文佳，苏建. 特高含水后期层系井网及注采优化方法与应用——以S油田T块为例. 天然气与石油. 2022(03): 56-61 .

Other cited types(2)

Get Citation

PDF

XML

Article Metrics

Article views (2608) PDF downloads (2999) Cited by(10)

Synthesis and Performance Evaluation of a Cement Retardant AID for Oil Well

Abstract

References

Related Articles

Cited by

Periodical cited type(8)

Other cited types(2)

Catalog

Article Metrics

Related

Synthesis and Performance Evaluation of a Cement Retardant AID for Oil Well

Abstract

References

Related Articles

Cited by

Periodical cited type(8)

Other cited types(2)

Catalog

Article Metrics

Related

Export File

Citation

Format

Content