李忠诚,鲍志东,王洪学,等. 基于高压汞灯荧光显微观测的剩余油定量分析方法[J]. 石油钻探技术,2024, 52(0):1-7. DOI: 10.11911/syztjs.2023114
引用本文: 李忠诚,鲍志东,王洪学,等. 基于高压汞灯荧光显微观测的剩余油定量分析方法[J]. 石油钻探技术,2024, 52(0):1-7. DOI: 10.11911/syztjs.2023114
Li Zhongcheng, Bao Zhidong, Wang Hongxue, et al. Quantitative Analysis Method of Residual Oil Based on Fluorescent Microscopic Observation of High Pressure Mercury Lamp[J]. Petroleum Drilling Techniques,2024, 52(0):1-7. DOI: 10.11911/syztjs.2023114
Citation: Li Zhongcheng, Bao Zhidong, Wang Hongxue, et al. Quantitative Analysis Method of Residual Oil Based on Fluorescent Microscopic Observation of High Pressure Mercury Lamp[J]. Petroleum Drilling Techniques,2024, 52(0):1-7. DOI: 10.11911/syztjs.2023114

基于高压汞灯荧光显微观测的剩余油定量分析方法

Quantitative Analysis Method of Residual Oil Based on Fluorescent Microscopic Observation of High Pressure Mercury Lamp

  • 摘要: 为明确不同驱油阶段微观剩余油的分布状态,指导老油田在注水开发后期的剩余油挖潜,选取典型区块不同级别渗透率岩心进行驱油试验,采用液氮冷冻技术制作岩心薄片并利用高压汞灯荧光显微镜分析饱和油阶段、水驱至模型初见水阶段和水驱结束后阶段的微观剩余油赋存状态。经过图像处理,将剩余油赋存状态细分为膜状、颗粒吸附状、角隅状、喉道状、簇状和粒间吸附状剩余油,并计算了不同状态剩余油的赋存比例。结果表明,中渗透率岩心水驱主要动用了自由态剩余油,水驱后残存的自由态剩余油较多,可作为继续挖潜对象;低渗透率岩心水驱过程中自由态微观剩余油含量进一步减少,水驱后束缚态的膜状剩余油及半束缚态的喉道状剩余油可作为接替开发对象。高压汞灯荧光显微观测法,为剩余油分析提供了一种新的量化方法,可以为老油田剩余油挖潜提供借鉴。

     

    Abstract: In order to determine the distribution state of micro residual oil in different oil displacement stages and guide the residual oil tapping strategy of old oilfields in the later stage of water injection development, cores with different levels of permeability in typical blocks are selected for oil displacement experiments, and the displacement stage is divided into three parts: saturated oil stage, water drive stage to the initial water stage of the model, and the stage after water drive, The liquid nitrogen freezing technology is used to make core slices and the high-pressure mercury lamp fluorescence microscope is used to analyze the microscopic remaining oil occurrence state in different displacement stages. After image processing, six types of remaining oil occurrence states are subdivided: membrane, particle adsorption, corner, throat, cluster and inter particle adsorption, The remaining oil proportion in different states was calculated. The water drive of medium permeability core mainly uses the free remaining oil. After water drive, there is more free remaining oil, which can be used as the object of further tapping potential; During water flooding of low permeability cores, the content of free micro residual oil is further reduced. After water flooding, bound membrane residual oil and semi bound throat residual oil can be used as replacement development objects. The fluorescence microscopic observation method of high-pressure mercury lamp provides a new quantitative method for residual oil analysis and reference for the residual oil tapping strategy of old oilfields.

     

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